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11.
《Ceramics International》2022,48(1):157-163
NASICON-type structured compounds Li1+xMxTi2-x(PO4)3 (M = Al, Fe, Y, etc.) have captured much attention due to their air stability, wide electrochemical window and high lithium ion conductivity. Especially, Li1.3Al0.3Ti1.7(PO4)3 (LATP) is a potential solid electrolyte due to its high ionic conductivity. However, its actual density usually has a certain gap with the theoretical density, leading the poor ionic conductivity of LATP. Herein, LATP solid electrolyte with series of SnO–P2O5–MgO (SPM, 0.4 wt%, 0.7 wt%, 1.0 wt%, 1.3 wt%) glass addition was successfully synthesized to improve the density and ionic conductivity. The SPM addition change Al/Ti–O bond and P–O bond distances, leading to gradual shrinkage of octahedral AlO6 and tetrahedral PO4. The bulk conductivity of the samples increases gradually with SPM glass addition from 0.4 wt% to 1.3 wt%. Both SPM and the second-phase LiTiPO5, caused by glass addition, are conducive to the improvement of compactness. The relative density of LATP samples increases first from 0 wt% to 0.7 wt%, and then decreases from 0.7 wt% to 1.3 wt% with SPM glass addition. The grain boundary conductivity also changes accordingly. Especially, the highest ionic conductivity of 2.45 × 10?4 S cm?1, and a relative density of 96.72% with a low activation energy of 0.34 eV is obtained in LATP with 0.7 wt% SPM. Increasing the density of LATP solid electrolyte is crucial to improve the ionic conductivity of electrolytes and SPM glass addition can promote the development of dense oxide ceramic electrolytes. 相似文献
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Lipase production by solid‐state fermentation of olive pomace in tray‐type and pressurized bioreactors 下载免费PDF全文
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井间是剩余油的主要分布区域,为探测井间剩余油,提高采收率,提出了基于全空间几何因子的瞬变电磁井间勘探方法。在本井使用线圈发射、邻井使用线圈接收,根据瞬变电磁场理论,在阶跃信号的激励下发射线圈在地层中激发出沿圆周方向的闭合瞬变电场,该电场在导电地层中产生与地层电导率呈正比的涡流。由Doll地层环模型可知,地层中的涡流在空间任意点激发得到与地层电导率成正比的二次场响应信号(有用信号),并可表示为空间各点电导率的加权平均值,其权重即为井间瞬变电磁勘探的全空间几何因子;全空间几何因子集中分布在发射线圈和接收线圈附近,其它区域分布较少,在发射线圈和接收线圈两侧呈现不同的极性;对瞬变电磁响应与地层电导率、井间距和源距的变化规律研究可知,瞬变电磁井间勘探有用信号随着地层电导率的增大而增大,随着井间距的增加单调减小,在发射线圈和接收线圈处于同一深度时该响应信号幅度最大。 相似文献
14.
Ashok Mahajan Naazneen Surti Pooja Koladiya 《Drug development and industrial pharmacy》2018,44(3):463-471
The aim of the present study was to improve the dissolution and flow properties of lurasidone hydrochloride (LH) by solid dispersion adsorbate (SDA) technique. Solid dispersions (SDs) of LH were prepared by fusion method using Poloxamer P188. The melt dispersion was adsorbed onto the porous carrier Florite (calcium silicate). A 32 factorial design was employed to quantify the effect of two independent variables, namely ratio of carrier (Poloxamer 188) and LH in SD and ratio of adsorbent (Florite) to SD. SDA granules of LH were studied for flow properties and characterized using differential scanning calorimetry, scanning electron microscopy, and X-ray diffraction. Tablets of optimized composition of SDA granules (equivalent to 20?mg of drug) and plain tablets were prepared by direct compression method. The dissolution studies were carried out in Mcllvaine buffer (pH 3.8) as per USFDA guidelines and characterized for parameters such as percent dissolution efficiency, t50, and Q30. Tablets prepared from SDA granules showed almost four-fold increase in cumulative percentage drug release as compared to tablets prepared from plain LH. The value of dissolution efficiency was enhanced from 49.60% for plain tablets to 94.15% for SDA tablets. SDA granules did not show any change in drug release and X-ray diffraction pattern after storage at 40?°C/75% of RH for 3?months, which confirms that Florite prevented conversion of drug from amorphous form to crystalline form improving physical stability of the amorphous state of LH. 相似文献
15.
Gerardo Valadez Huerta Johanan Álvarez Jordán Michael Dragon Keno Leites Stephan Kabelac 《International Journal of Hydrogen Energy》2018,43(34):16684-16693
Solid oxide fuel cell (SOFC) systems with anode off-gas recirculation (AGR) and diesel pre-reforming are advantageous because they can operate with the current fuel infrastructure. In the SchIBZ-project, the prototype of such a SOFC system for maritime applications has already been commissioned. In this first paper, we model the system devices to conduct an exergy analysis of this real SOFC plant and validate them with experimental values from experiments in laboratory scale. The results of our simulation agree well with the experimental values. The calculations with the validated results may be closer to the real thermodynamic behavior of such system components than previous literature. 相似文献
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针对未考虑正偏心正交车铣切削层几何形状而导致难以全面反映正交车铣切削层几何形状变化规律的问题,基于正交车铣运动规律,在不考虑动力学影响的情况下,对切削层的形成过程进行了静态分析。建立的正偏心正交车铣切削层几何形状的解析模型涉及铣刀侧刃和底刃的切入/切出角度、切削厚度和切削深度。通过试验验证了该解析模型的正确性,并分析了切削参数对铣刀切削层的影响。研究结果为正偏心正交车铣切削层几何形状的变化提供了定量的分析依据,为切削力和颤振的研究提供了理论指导。 相似文献
19.
Moritz Riebisch Philipp Weiß Clemens Cremer Ibrahim Aboulkhair Andreas Bührig-Polaczek 《Materials Science & Technology》2018,34(6):725-730
Solid solution-strengthened ductile iron (DI) exhibits outstanding mechanical properties due to the high silicon content. The strengthening by silicon addition is limited since additions above 4.3?wt-% lead to embrittlement. For a further improvement of mechanical properties, other alloying elements need to be considered. In the present work, the effect of various copper additions on the microstructure and the mechanical properties of solid solution-strengthened DI were investigated. The results show that no appreciable strengthening can be achieved by copper addition without the formation of pearlite in the matrix. The pearlite content increases considerably for Cu-additions above 0.23?wt-% and is independent of the cooling rate for the cooling conditions analysed. 相似文献
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